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We typically use a blood test to determine this

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Condensation matters because any moisture on the stopper can alter the actual solvent volume you introduce, creating concentration inconsistencies from the very first step

J Agr Food Sci 52:41924196 Zhang D, Xie P, Chen J, Dai M, Qiu T, Liang G (2009) Determination of microcystin-LR and its metabolites in snail ( Bellamya aeruginosa ), shrimp ( Macrobrachium nipponensis ) and silver carp ( Hypophthalmichthys molitrix ) from Lake Taihu, China